The system consists of four separate parts:
- A cylindrical vacuum chamber with an integrated sample stage for thermal conductivity measurements, mounted on a floor-stand.
- A helium gas compressor requiring water cooling with a capacity >6.5 kW.
- A temperature control unit.
- A turbomolecular pump.
The exterior of the vacuum chamber is made of stainless steel, while the interior – mainly the sample holder used for thermal conductivity measurement – is made of copper, with heat conduction established via copper belts. Sample mounting is made easily accessible by loosening the bolt connections on the chamber lid and lifting the cylindrical lid upward. The feedthroughs for both TPS and temperature-measurement cables are located on the top of the chamber, terminating in a hermetic connector. The chamber can reach temperatures as low as 5 K (-268°C), with a temperature stability of ±0.1 K (±0.1°C).
The cryostat is designed to be used with our Kapton- or Teflon-insulated Hot Disk® or Hot Strip® sensors equipped with thin-diameter silicone-clad cables, minimizing heat leakage into the vacuum chamber through the sensor leads.
Initial evacuation of the chamber, followed by activation of the helium compressor for gas circulation, is performed manually. Subsequent chamber temperature control is handled by the resistive heating element and fully automated via the Hot Disk Desktop App over USB communication. The software can be programmed to execute a series of measurements with the Hot Disk instrument at multiple chamber temperatures.
| Size | |
|---|---|
| Volume | 4.5 liters |
| Height | 210 mm |
| Diameter | 230 mm |
| Maximum sample size | |
| Thickness | 45 mm (one of two identical pieces) |
| Width | 100 mm |
| Length | 100 mm |
| Vacuum level | 0.03 mbar |
| Cooling system | Helium gas, closed cycle |
| Heating system | Wire heating element |
| Temperature | |
| Minimum | 5 K (-268°C) |
| Maximum | Room temperature |
| Stability | ±0.1 K (±0.1°C) |
| Compressor | |
|---|---|
| Helium | 2.5 ounce |
| Helium flow | ~50 litres/min at ~1.7 MPa |
| Water cooling | >6.5 kW |
| Supply voltage | |
| Temperature control unit | 230 VAC, 50/60 Hz, 1 Phase |
| Turbomolecular pump | 100-230 VAC, 50/60 Hz, 1 Phase |
| Compressor | 360-480 VAC, 50/60 Hz, 3 Phase |
| Power rating | |
| Temperature control unit | |
| Turbomolecular pump | 1.7/0.85 A |
| Compressor | Min. circuit ampacity 17 A |
| Input/output | |
| Temperature control unit | USB type B connector (female) |
| Dimensions (height x width x depth) | |
| Vacuum chamber (with floor-stand) | 1470 mm x 600 mm x 600 mm |
| Temperature control unit | 100 mm x 220 mm x 380 mm |
| Turbomolecular pump | 320 mm x 400 mm x 350 mm |
| Compressor | 591 mm x 450 mm x 485 mm |
| Weight | |
| Temperature chamber (with floor-stand) | 76 kg |
| Temperature control unit | 3 kg |
| Turbomolecular pump | 17 kg |
| Compressor | 120 kg |
| CE marking | In progress |